Reuse & Permissions

It is not necessary to obtain permission to reuse this article or its components as it is available under the terms of the Creative Commons Attribution 4.0 International license. This license permits unrestricted use, distribution, and reproduction in any medium, provided attribution to the author(s) and the published article's title, journal citation, and DOI are maintained. Please note that some figures may have been included with permission from other third parties. It is your responsibility to obtain the proper permission from the rights holder directly for these figures.

Export citation

Export citation

Choose format for download:

Download Citation
  • Open Access
  • Access by Xinjiang University

Rheological measurements on dense suspensions containing dendrite-like particles

Andreas Ludwig, Mihaela Stefan-Kharicha, Christian Gomes Rodrigues, Johann Mogeritsch, Menghuai Wu, and Abdellah Kharicha

Phys. Rev. E 114, 015417 – Published 22 July, 2026

DOI: https://doi.org/10.1103/nmkb-mj7x

Abstract

During alloy solidification, equiaxed dendrites often move within the solidifying liquid. As this motion is one of the main causes of macrosegregation, a deeper understanding of the behavior of suspensions containing dendrite-like particles is particularly important. Inspired by rheological investigations with dense suspensions containing spheres, pressure-imposed rheological measurements using an annular shear cell were performed and applied to suspensions containing 3D-printed dendrite-like particles. The results indicate that the concept of the friction coefficient for spheres can be adapted by using appropriate coefficients and suitably reduced mechanical coherency limits. Consequently, the particle pressure of interacting, moving dendrite-like particles in liquids can be effectively described. However, direct measurement of the shear rate was not possible due to the shallowness of the rheological cell used. Nevertheless, the viscosity of suspension containing dendrite-like particles could be estimated indirectly by adapting the dimensionless friction number originally proposed for suspensions with spheres. An increase in viscosity at the same reduced solid fraction, due to the specific morphology of the dendrite-like particles, is predicted. While spheres predominantly interact by sliding past one another, dendrite-like particles—particularly those with long sidearms—interact mainly through rotation.

View figure in article

Physics Subject Headings (PhySH)

Article Text

References (31)

  1. W. Kurz and D. J. Fisher, Fundamentals of Solidification, 4th ed. (Trans. Tech. Publ., Aedermansdorf, 1998).
  2. J. A. Dantzig and M. Rappaz, Solidification, 2nd ed. (EPFL Press, Lausanne, 2016).
  3. M. Torabi Rad, M. Založnik, H. Combeau, and C. Beckermann, Upscaling mesoscopic simulation results to develop constitutive relations for macroscopic modeling of equiaxed dendritic solidification, Materialia 5, 100231 (2019).
  4. G. Zimmermann, L. Sturz, Y. Z. Li, C. Gandin, R. Fleurisson, C. Beckermann, and A. Karma, Columnar and equiaxed solidification of Al-7 wt.% Si alloys in reduced gravity in the framework of the CETSOL project, JOM online 69, 1269 (2017).
  5. K. Fezi, A. Plotkowski, and M. J. Krane, Macrosegregation modeling during direct-chill casting of aluminum alloy 7050, Num. Heat Transf. A 70, 939 (2016).
  6. H. C. de Groh III, P. D. Weidman, R. Zakhem, S. Ahuja, and C. Beckermann, Calculation of dendrite settling velocities using a porous envelope, Met. Trans. B 24, 749 (1993).
  7. S. Gerardin, H. Combeau, and G. Lesoult, Étude de l'effet du mouvement relatif cristal/liquide sur la croissance d'un cristal dendritique dans un liquide en surfusion, J. Phys. IV 11, Pr6-143 (2001).
  8. A. Badillo, D. Ceynar, and C. Beckermann, Growth of equiaxed dendritic crystals settling in an undercooled melt, Part 1: Tip kinetics, J. Cryst. Growth 309, 197 (2007).
  9. A. Badillo, D. Ceynar, and C. Beckermann, Growth of equiaxed dendritic crystals settling in an undercooled melt, Part 2: Internal solid fraction, J. Cryst. Growth 309, 216 (2007).
  10. A. Olmedilla, M. Založnik, B. Rouat, and H. Combeau, Packing of sedimenting spherical and equiaxed non-convex particles, Phys. Rev. E 97, 012910 (2018).
  11. J. Ni and C. Beckermann, A volume-averaged two-phase model for transport phenomena during solidification, Met. Trans. B 22, 349 (1991).
  12. C. Beckermann and R. Viskanta, Mathematical modeling of transport phenomena during alloy solidification, Appl. Mech. Rev. 46, 1 (1993).
  13. I. M. Krieger and T. J. Dougherty, A mechanism for non-newtonian flow in suspensions of rigid spheres, Trans. Soc. Rheol. 3, 137 (1959).
  14. I. M. Krieger, Rheology of monodisperse latices, Adv. Colloid Interface Sci. 3, 111 (1972).
  15. A. Ludwig and M. Wu, Modeling of globular equiaxed solidification with a two-phase approach, Met. Mater. Trans. A 33, 3673 (2002).
  16. M. Wu, A. Ludwig, A. Bührig-Polaczek, M. Fehlbier, and P. R. Sahm, Influence of convection and grain movement on globular equiaxed solidification, Int. J. Heat Mass Transf. 46, 2819 (2003).
  17. T. Wang, M. Wu, A. Ludwig, M. Abondano, B. Pustal, and A. Bührig-Polaczek, Modelling the thermosolutal convection, shrinkage flow and grain movement of globular equiaxed solidification using a three phase model, Int. J. Cast Met. Res. 18, 221 (2005).
  18. C. Y. Wang and C. Beckermann, Equiaxed dendritic solidification with convection Part I: Multiscale/multiphase modeling, Met. Mater. Trans. A 27, 2754 (1996).
  19. C. Y. Wang and C. Beckermann, Part II: Numerical simulations for an AI-4 Wt Pct Cu alloy, Met. Mater. Trans. A 27, 2765 (1996).
  20. M. Wu and A. Ludwig, Modeling equiaxed solidification with melt convection and grain sedimentation—I: Model description, Acta Mater. 57, 5621 (2009).
  21. M. Wu and A. Ludwig, Modeling equiaxed solidification with melt convection and grain sedimentation—II. Model verification, Acta Mater. 57, 5632 (2009).
  22. A. K. Dahle and D. H. StJohn, Rheological behaviour of the mushy zone and its effect on the formation of casting defects during solidification, Acta Mater. 47, 31 (1998).
  23. I. Farup and A. Mo, Two-phase modeling of Mushy zone parameters associated with hot tearing, Met. Mater. Trans. A 31, 1461 (2000).
  24. A. K. Dahle and L. Arnberg, Development of strength in solidifying aluminium alloys, Acta Mater. 45, 547 (1997).
  25. M. Wu, A. Fjeld, and A. Ludwig, Modelling mixed columnar-equiaxed solidification with melt convection and grain sedimentation–Part I: Model description, Comp. Mater. Sci. 50, 32 (2010).
  26. T. Haxhimali, A. Karma, F. Gonzales, and M. Rappaz, Orientation selection in dendritic evolution, Nat. Mater. 5, 660 (2006).
  27. F. Boyer, E. Guazzelli, and O. Pouliquen, Unifying suspension and granular rheology, Phys. Rev. Lett. 107, 188301 (2011).
  28. DOI: 10.34901/mul.pub.2026.036.
  29. A. Einstein, Eine neue bestimmung der moleküldimensionen, Ann. Phys. 324, 289 (1906).
  30. A. Einstein, Berichtigung zu meiner arbeit: eine neue bestimmung der moleküldimensionen, Ann. Phys. 339, 591 (1911).
  31. É. Guazzelli and O. Pouliquen, Rheology of dense granular suspensions, J. Fluid Mech. 852, 1 (2018).

Outline

Information

Sign In to Your Journals Account

Filter

Filter

Article Lookup

Enter a citation